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<div id="35hf15jpnp" class="NyNewsdetail_con"> <p><span style="font-family:宋體"> 常用的電極法<strong>氨氮分析儀</strong>分為氨氣敏電極法和電導法等，其中氨氣敏電極法技術比較成熟，應用較廣。</span></p><p><span style="font-family:宋體"> <img alt="" src="http://img71.chem17.com/9/20190708/636981801689880588371.png" style="height:377px; width:243px" /></span></p><p><span style="font-family:宋體">氨氣敏電極法</span></p><ol><li><span style="font-family:宋體">儀器的工作原理</span> <span style="font-family:宋體">將水樣導人測量池中，加人氫氧化鈉使水樣中離子態(tài)銨轉(zhuǎn)換為游離態(tài)氨，游離態(tài)氨透過氨氣敏電極的憎水膜進人電極內(nèi)部緩沖液，改變緩沖液的</span>pH<span style="font-family:宋體">值，儀器通過測量</span>pH<span style="font-family:宋體">值變化即可測量水樣中的氨濃度。</span></li></ol><p><span style="font-family:宋體"> 氨氣敏電極法結(jié)構(gòu)簡單、試劑用量少、測量范圍寬，但電極穩(wěn)定性較差，膜電極容易受污染，對環(huán)境溫度要求較高。目前采用氣敏電極法的<strong>氨氮分析儀</strong>主要有德國</span> WTW<span style="font-family:宋體">、河北先河等公司的產(chǎn)品。</span></p><p><span style="font-family:宋體"> 儀器采用氨氣敏電極對水中的氨氮進行測試。</span> <span style="font-family:宋體">氨氣敏電極包括平頭的</span><strong>pH<span style="font-family:宋體">玻璃電極</span></strong><span style="font-family:宋體">和銀</span>/<span style="font-family:宋體">氯化銀電極，兩支電極通過含有銨離子的內(nèi)允液被組裝在一起，作為這</span>pH<span style="font-family:宋體">值側(cè)量電對。內(nèi)充液是</span>0. lmol/L<span style="font-family:宋體">的氯化氨溶液，通過氣透膜與樣品隔開。當把電極浸入加有試劑的待測液中時，待測液中的離子態(tài)錢變?yōu)橛坞x態(tài)氨，隨同待測液中的游離態(tài)氨一同通過氣透膜進入內(nèi)充液，使內(nèi)充液的</span>pH<span style="font-family:宋體">值發(fā)生變化，并產(chǎn)生與樣品濃度的對數(shù)呈正比的電壓變化信號。</span></p><p><span style="font-family:宋體"> 監(jiān)測儀由進樣系統(tǒng)</span>(<span style="font-family:宋體">兩位三通閥、雙通道蠕動泵</span>)<span style="font-family:宋體">、控制系統(tǒng)</span>(<span style="font-family:宋體">工控機等</span>)<span style="font-family:宋體">、測試系統(tǒng)</span>(<span style="font-family:宋體">氨氣敏電極、模數(shù)轉(zhuǎn)換</span>)<span style="font-family:宋體">、顯示系統(tǒng)</span>(<span style="font-family:宋體">液晶顯示屏</span>)<span style="font-family:宋體">及附件等組成。</span></p><p><span style="font-family:宋體">主要技術指標。</span></p><ul><li><span style="font-family:宋體">測量范圍：</span> 0.0<span style="font-family:宋體">5</span><span style="font-family:宋體">～</span>1000 mg/L<span style="font-family:宋體">。</span></li><li><span style="font-family:宋體">重現(xiàn)性：≤</span>3%<span style="font-family:宋體">。</span></li><li><span style="font-family:宋體">零點漂移</span><span style="font-family:宋體">:</span><span style="font-family:宋體">±0.5mg/L。</span></li><li><span style="font-family:宋體">量程漂移：</span><span style="font-family:宋體">±</span>4%F.S<span style="font-family:宋體">。</span></li><li><span style="font-family:宋體">響應時間</span><span style="font-family:宋體">：＜</span>4 min<span style="font-family:宋體">。</span></li><li><span style="font-family:宋體">示值誤差：相對誤差小于</span><span style="font-family:宋體">±</span>10 %<span style="font-family:宋體">。</span></li></ul> </div> <div id="35hf15jpnp" class="ly_PrevNext"> <ul> <li>上一篇：<a href="/szhcy-Article-1891505/">工業(yè)廢水有哪些分類？</a></li> <li>下一篇：<a href="/szhcy-Article-1889152/">玻璃電極法的原理</a></li> </ul> </div> </div>   <div id="35hf15jpnp" class="foot_box"> <div 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